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MDPI AG
Two Isomers of a Novel Ag(I) Complex with Pyrazole-Type Ligand—Synthesis, Structural, Thermal, and Antioxidative Characterization
The synthesis of the first Ag(I) complexes with ethyl-5-amino-1-methyl-1H-pyrazole-4-carboxylate (L) is presented. The reaction of AgClO4 with the ligand in a molar ratio of 1:1 gives a bis(ligand) complex [AgL2]ClO4 (1) in the presence of 4-formylbenzonitrile, monoperiodic polymer {[AgL2]ClO4}n (2). Characterization involved IR spectroscopy, conductometric measurements, thermogravimetric analysis, antioxidant tests, powder, and single crystal X-ray diffraction. Structural analysis revealed ligand...
Download 2023 Nikola D. Radnović , Željko K. Jaćimović , Mirjana M. Radanović , Ivana Đ. Borišev , Berta Barta Holló , Marko V. Rodić , Nađa Štetin
Walter de Gruyter GmbH
Crystal structure of 3-(4-bromophenyl)-5-methyl-1H-pyrazole, C10H9BrN2
Abstract C10H9BrN2, orthorhombic, P212121 (no. 19), a = 5.9070(3) Å, b = 9.2731(7) Å, c = 17.5641(14) Å, V = 962.09(12) Å3, Z = 4, Rgt (F) = 0.0504, wRref (F 2) = 0.0947, T = 293(2) K.
Download 2023 Zoran D. Tomić , Željko K. Jaćimović , David Kočović , Snezana Mugosa , Sergiu Shova
Walter de Gruyter GmbH
Crystal structure of 4-bromo-3-nitro-1H-pyrazole-5-carboxylic acid monohydrate, C4H2N3BrO4·H2O
Abstract C4H2N3BrO4·H2O, monoclinic, P21/c (no. 14), a = 7.177(2) Å, b = 10.999(3) Å, c = 10.414(3) Å, β =  100.145 ( 11 ) ∘...
Download 2023 Zoran D. Tomić , Ana Radović , Željko K. Jaćimović , David Kočović , Gerald Giester
Wiley
Construction of Sensor for Submicromolar Detection of Riboflavin by Surface Modification of SPCE with Thermal Degradation Products of Nickel Acetate Tetrahydrate
AbstractNickel acetate tetrahydrate (NAT) sample series were used to modify screen‐printed carbon electrodes (SPCE). The samples were hybrid Ni/NiO nanocomposites, where the NiO phase increased with an applied treatment temperature. Results of electrochemical measurements pointed that the Ni/NiO550/SPCE‐modified electrode had the best analytical performance toward the detection of riboflavin (RF). The Ni/NiO550/SPCE‐based sensor showed linear response with RF in the concentration range of 0.5–75 μM...
Download 2022 Milica Kosović‐Perutović , Svetozar Musić , Bratislav Antić , Dalibor M. Stanković , Željko K. Jaćimović , José F. M. L. Mariano , Stjepko Krehula , Miloš Ognjanović
Walter de Gruyter GmbH
The crystal structure of bis[4-bromo-2-(1H-pyrazol-3-yl) phenolato-κ2 N,O] copper(II), C18H12Br2CuN4O2
Abstract C18H12Br2CuN4O2, monoclinic, P21/c (no. 14), a = 11.5165(11) Å, b = 5.4369(5) Å, c = 14.4872(14) Å, V = 873.52(14) Å3, Z = 2, R gt (F) = 0.0232, wR ref (F 2) = 0.0559, T = 200 K.
Download 2021 Zoran D. Tomić , Željko K. Jaćimović , Gerald Giester , Atifa Ajanović , Eugen Libowitzky , Milica Kosović
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