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National Library of Serbia
First cobalt complexes with methyl pyruvate semi/thiosemicarbazone - synthesis, physico-chemical and structural characterization
In the reaction of acetone solutions of CoX2?nH2O (X = Cl, Br) with methyl pyruvate semi/thiosemicarbazone (Hmps, Hmpt) the first Co(II) complexes with these ligands, i.e., [Co(Hmps)(H2O)X2] (X = Cl (1), Br (2)), [Co(Hmpt)2][CoCl4]?2H2? (3) and [Co(Hmpt)2]Br2?Me2CO (4) were obtained. Complexes 1 and 2 represent the first examples of metal complexes of Hmps. All the obtained compounds were characterized by elemental analysis, conductometry, magnetic measurements, and IR spectra, and for complexes...
Download 2020 Ljiljana Vojinovic-Jesic , Željko Jaćimović , Vukadin Leovac , Mirjana Radanovic , Vukoslava Miskov-Pajic , Vukosava Zivkovic-Radovanovic , Marko Rodic , Svetlana Belosevic
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